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題名 | Synthesis, Crystal Structure and Magnetic Property of Diiron Complex [Fe(phen)[feb0]][Fe[feaf]OCI[feb8]].2CH[feb0]CN |
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作者姓名(中文) | 閆冰; 陳志達; 王詩璽; | 書刊名 | Journal of the Chinese Chemical Society |
卷期 | 47:6 2000.12[民89.12] |
頁次 | 頁1211-1214 |
分類號 | 346.01 |
關鍵詞 | 合成; 晶體結構; Synthesis; Crystal structure; Variable-temperature susceptibility; Diron complex; |
語文 | 英文(English) |
英文摘要 | A new diiron complex has been synthesized and characterized by X-ray single crystal structural analysis: [FeII(phen)3][FeIII2OCl6]�R��2CH3CN. The complex crystallizes in the monoclinic system, space group C2/c, with lattice parameters a = 21.162(4) A, b = 15.168(3) A, c = 14.812(3) A, �� = 112.71 (3)�S��, V = 4385.8(15) A3, Dx = 1.543 Mg/m3, Z = 4. The corresponding variable temperature susceptibility measurement shows that there exists an antiferromagnetic interaction in the complex. |
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