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題名 | 人參類藥材中抗黴菌劑之調查(2)=Survey of Fungicide Residues in Ginseng (Ⅱ) |
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作者 | 賴齡; 曾信雄; 溫國慶; Lay, Ling; Tseng, Hshinn-hshiung; Wen, Kuo-ching; |
期刊 | 藥物食品檢驗局調查研究年報 |
出版日期 | 19971100 |
卷期 | 15 1997.11[民86.11] |
頁次 | 頁111-118 |
分類號 | 418.5 |
語文 | chi |
關鍵詞 | 人參類藥材; 抗黴菌劑; HPLC; Thiabendazole; O-phenylphenol; Biphenyl; GC/ECD; CS[feaf]; CCl[feb2]; |
中文摘要 | 人參因含糖量及含水量高,因此容易因環境因子之影響而導致黴菌之滋生,甚至 產毒影響中藥材之安全性。為瞭解廣泛使用之粉光參藥材,在販售前是否噴灑,燻蒸或添加 抗黴菌劑,以防止黴菌之滋長及破壞。以逢機取機方式,抽購60件粉光參,以HPLC之方法分 析TBZ(Thiabendazole),OPP(O-phenylphenol),BP(Biphenyl)及GC/ECD之方法分析 CS�砥ACC1�瓷A結果均未檢出。另TBZ,OPP,BP各添加20∼80 ug之平均回收率分別為60.3% ,78.8%,86.2%,最低檢出量分別為 1ppm,0.75 ppm,0.75 ppm,CS�砥ACC1�略坏郁〃K加 回收率分別為61.2%,82.5%,最低檢出量分別為0.5 ppm,0.03 ppm,在檢測範圍內具有良 好的線性關係。藥材經CS�砥ACC1�笨t蒸後,在其最低之檢測範圍,均可檢出其含量。 |
英文摘要 | Multiresidue analysis methods using HPLC and GC/ECD were used to analyze the thiabendazole (TBZ), o-phenylpheonl (OPP), biphenyl (BP),CS�畝nd CC1�淆ontent in Panacis Quinquefoli Radix. The average recoveries of TBZ, OPP and BP were 60.3, 78.8 and 86.2% at 20, 40 and 80 ug fortification levels, respectively and the detection limits were 1, 0.75 and 0.75 ppm. The average recoveries of CS�畝nd CC1�琅ere 61.2 and 82.5% and the detection limits were 0.5, 0.03 ppm, respectively. Linear regression analysis gave good linear relationships. Sixty samples of Panacis Quinquefolii Radix were analyzed, but none of the samples were detectable. |
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