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題名 | Low-Temperature Synthesis of Monoclinic Celsian via a Citrate-Nitrate Reaction Process=檸檬酸法低溫合成單斜鋇長石粉體 |
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作者 | 林鑫龍; 黃啟輝; 蔣瑞光; 林文豪; 李維特; | 書刊名 | 遠東學報 |
卷期 | 26:4 2009.12[民98.12] |
頁次 | 頁553-562 |
分類號 | 440.33 |
關鍵詞 | 鋇長石; 檸檬酸法; 粉體; Monocelsian; Citrate process; Powder; |
語文 | 英文(English) |
中文摘要 | 本研究利用檸檬酸凝膠法合成計量型單斜鋇長石 BaAl2Si2O8 (BAS)粉 體。實驗將硝酸鋇、硝酸鋁、硝酸鋰、矽溶膠、檸檬酸和二乙二醇混合形 成透明溶膠再經乾燥後形成易於處理之粉體。粉體之特性分別以 XRD, DTA,TGA 和 TMA 加以分析。由 XRD 結果顯示添加 0.20 mole 硝酸鋰之 前驅體可於 850 oC– 900 oC 恆溫 4 小時後則可完全轉變為單斜鋇長石相。 |
英文摘要 | A citrate-nitrate process was successfully used to prepare a monoclinic celsian powder with the stoichiometric composition of BaAl2Si2O8 (BAS). The solutions of barium, aluminum and lithium nitrates, colloidal silica, citric acid, and diethylene glycol were combined and afforded a clear gel on mixing which was further decomposed on heating to an easily handled precursor in a powder form. The characteristics of this dried precursors were analyzed by X-ray powder diffraction (XRD), differential thermal analysis (DTA) and thermal gravimetric analysis (TGA), thermal mechanical analysis (TMA), respectively. BAS precursor doped with 0.2 mole LiNO3 would reach full conversion of hexacelsian-to-monocelsian in the temperature range of 850 oC – 900 oC after 4-hour calcinations. |
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