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題名 | 雜環系嘧啶賽安寧和氮次甲基染料之合成及其性質之研究=Synthesis and Characteristics of Cyanine and Azomethine Dyes Synthesized from 3-Cyano-4-methyl-6-phenyl-2(1H)-pyrimidinethione |
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作者 | 顏明賢; 程曉鳳; 蔡馨輝; | 書刊名 | 紡織中心期刊 |
卷期 | 13:3 2003.07[民92.07] |
頁次 | 頁262-274 |
分類號 | 465.3 |
關鍵詞 | 嘧啶; 賽安寧染料; 氮次甲基染料; Pyrimidinethione; Cyanine dayes; Azomethine dyes; |
語文 | 中文(Chinese) |
中文摘要 | 本文研究主傲合成雜環系嘧啶染料,利用異氰酸銨、氯化苯甲醯和3-氨基丁烯氰三者在溶劑1.4-二氧陸圜下加熱迴流反應合成得中間體3-Cyano-4-methyl-6-phenyl-2(1H)-pyrimidinethior時,進而與氯氰基基甲烷行縮合反應得中間體5-Amino-4-methyl-2-phenylthieno[2,3-d]pyrimidine-6-carbonitrile ,再與偶合鹽在冰浴下行偶合反應,合成一系列雜環系嘧啶染料。所合成之染料皆經光譜儀測定分析其構造,進而對聚酯織物與聚醯胺織物行染色,探討染織物之上色性、均染性及染色堅牢度。 |
英文摘要 | A series of heterocyanine and heteroazomethine dyes were synthesized 3-cyano- 4-methyl-6-phenyl-2(1H)-pyrimidinethione and 5-amino-4methyl- 2-phenyl-thieno[2,3-d] pyrimidine-6-carbonitrile have been synthesized. Characteization of thes dyes were carried out by spectral and their dyeing properties measured were also studied. |
本系統之摘要資訊系依該期刊論文摘要之資訊為主。