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題名 | Determination of Aldicarb, Propoxur, Carbofuran, Carbaryl and Methiocarb Residues in Honey by HPLC with Post-column Derivatization and Fluorescence Detection after Elution from A Florisil Column=利用HPLC配合後柱衍生反應及矽酸鎂管柱沖提後螢光偵測分析蜂蜜中Aldicarb、Propoxur、Carbofuran、Carbaryl及Methiocarb之農藥殘量 |
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作者姓名(外文) | Koc, Feride; Yigit, Yusuf; Das, Yavuz Kursad; Gurel, Yasemin; Yarali, Cevdet; | 書刊名 | 藥物食品分析 |
卷期 | 16:3 2008.06[民97.06] |
頁次 | 頁39-45+91 |
分類號 | 412.3 |
關鍵詞 | 蜂蜜; 液相層析; 後柱衍生反應; 含氮甲基胺基甲酸鹽農藥; 殘留; 矽酸鎂; Honey; Liquid chromatography; Post-column derivatization; N-methylcarbamate pesticide; Residue; Florisil; |
語文 | 英文(English) |
英文摘要 | The aim of this study was to develop an easy analytical method for determining aldicarb, propoxur, carbofuran, carbaryl and methiocarb residues in honey by high performance liquid chromatography with post-column derivatization and fluorescence detection (HPLC/PCD-FL) for routine analysis. A florisil packed column was used in sample preparation step and showed good performance. The recoveries ranged between 72.02 and 92.02% for various spiking levels (50, 100, 200 ng/g). The limits of detection were 4–5 ng/g, depending on different N-methylcarbamate pesticides. The extraction method used in the present study was easy, inexpensive, and rapid. Thus, it could be used efficiently in the routine monitoring studies. |
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